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Reduce Fe ₂ O ∝ to below 20ppm: Application of Shandong Heavy Industry's calcination, acid washing, flotation, and magnetic separation in high-purity sand

2026-06-15

High purity quartz sand has extremely strict requirements for Fe ₂ O Ⅲ content, gas-liquid inclusion quantity, and product whiteness. Shanlu Heavy Industry provides a complete set of purification equipment from calcination water quenching to acid washing, flotation, and electromagnetic slurry magnetic separation, suitable for the production of photovoltaic quartz sand, high-purity quartz sand, and high-end board sand.

Taking a typical high-purity purification process route as an example: After crushing and grading the raw ore, it is first sent to a calcination furnace for high-temperature heat treatment. The calcination furnace designed by Shanlu Heavy Industry is a rotary structure, and the furnace tube is made of heat-resistant stainless steel or corundum material. The working temperature can be set between 800 ℃ and 1100 ℃. The sand material rolls forward in the furnace and is uniformly heated, which can cause the gas-liquid inclusions inside the quartz particles to expand and break due to heat, while also promoting the diffusion of impurity elements in the lattice to the surface. The calcined sand quickly enters the cold water tank for water quenching, and the thermal stress generated by rapid cooling causes minerals to crack along the interface, which is beneficial for subsequent grinding and impurity dissociation.

After water quenching, the sand material is dehydrated and sent to the acid washing reaction kettle for chemical leaching. The pickling reaction kettle is made of 304 stainless steel lined with polytetrafluoroethylene or enamel material, which is resistant to strong acid corrosion. The kettle is equipped with a steam heating jacket and an anchor stirrer, which can achieve single acid or mixed acid leaching of hydrochloric acid, oxalic acid, hydrofluoric acid, etc. The reaction temperature is controlled between 60 ℃ and 90 ℃, and the leaching time can be adjusted between 2-6 hours. After acid washing, the sand material can be neutralized, cleaned, and dehydrated, and the Fe ₂ O3 content can be reduced to below 30ppm.

For quartz sand containing silicate impurities such as feldspar and mica, flotation purification is required after acid washing. Shanlu Heavy Industry uses SCF flotation machine and adopts acidic or alkaline flotation process. By adding amine collectors, impurities such as feldspar adhere to the bubbles and float, while quartz remains at the bottom of the tank. The flotation machine adopts a DC tank body, and the suction volume can be controlled by adjusting the gap between the stator and rotor. The flotation concentration is 25% -35%, and quartz concentrate with a purity of over 99.5% can be obtained.

Fine iron and titanium minerals may still remain in the flotation fine sand, requiring further magnetic separation. Shanlu Heavy Industry is equipped with a DCJ electromagnetic slurry magnetic separator at this stage. The device adopts electromagnetic excitation, with a background field strength of up to 15000Gs. The sorting chamber is filled with a magnetic medium, and weak magnetic particles are captured by the medium when the slurry flows through. The DCJ magnetic separator is suitable for fine ore slurry with a mesh size of -200 or more, accounting for over 80%. During continuous operation, it can reduce the Fe ₂ O Ⅲ content to below 20ppm, meeting the requirements of first-class photovoltaic quartz sand. The equipment is equipped with an automatic backwash system, which can be cleaned online after the medium is blocked without stopping the machine.

The above unit equipment can be centrally controlled by PLC. Shanlu Heavy Industry is located in Shandong and has over 20 years of experience in mining machinery design. Its products cover a full range of categories including calcination, acid washing, flotation, magnetic separation, dehydration, and drying. Shanlu Heavy Industry can provide customized process solutions based on the customer's original quartz grade and inclusion characteristics.

In terms of equipment details, the calcination furnace cylinder adopts a high-temperature resistant sealing structure with high thermal efficiency; The acid washing reaction kettle is equipped with an acid mist absorption tower, which meets environmental protection requirements; The impeller of the flotation machine is covered with wear-resistant rubber, which has a long service life; The electromagnetic slurry magnetic separator adopts water and electricity separation cooling, with stable temperature rise control. These designs reduce customer operational risks.

If you need equipment selection or incoming material testing data for high-purity quartz sand purification line, please call Manager Zhang at 13583776655 (same as WeChat).


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